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Fabrication and catalytic performance of meso-ZSM-5 zeolite encapsulated ferric oxide nanoparticles for

Zhenheng Diao, Lushi Cheng, Wen Guo, Xu Hou, Pengfei Zheng, Qiuyueming Zhou

《化学科学与工程前沿（英文）》 2021年 第15卷 第3期   页码 643-653 doi: 10.1007/s11705-020-1972-3

摘要： An encapsulation-structured Fe O @meso-ZSM-5 (Fe@MZ5) was fabricated by confining Fe O nanoparticles (ca. 4 nm) within the ordered mesopores of hierarchical ZSM-5 zeolite (meso-ZSM-5), with ferric oleate and amphiphilic organosilane as the iron source and meso-porogen, respectively. For comparison, catalysts with Fe O (ca. 12 nm) encapsulated in intra-crystal holes of meso-ZSM-5 and with MCM-41 or ZSM-5 phase as the shell were also prepared via sequential desilication and recrystallization at different pH values and temperatures. Catalytic phenol hydroxylation performance of the as-prepared catalysts using H O as oxidant was compared. Among the encapsulation-structured catalysts, Fe@MZ5 showed the highest phenol conversion and hydroquinone selectivity, which were enhanced by two times compared to the Fe-oxide impregnated ZSM-5 (Fe/Z5). Moreover, the Fe-leaching amount of Fe@MZ5 was only 3% of that for Fe/Z5. The influence of reaction parameters, reusability, and ·OH scavenging ability of the catalysts were also investigated. Based on the above results, the structure-performance relationship of these new catalysts was preliminarily described.

关键词： phenol hydroxylation     encapsulation structure     structure-performance relationship     meso-ZSM-5     ferric oxide    

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Thermal decomposition mechanism of ammonium sulfate catalyzed by ferric oxide

Xingfu SONG, Jingcai ZHAO, Yunzhao LI, Ze SUN, Jianguo YU

《化学科学与工程前沿（英文）》 2013年 第7卷 第2期   页码 210-217 doi: 10.1007/s11705-013-1320-y

摘要： The decomposition mechanism of ammonium sulfate catalyzed by ferric oxide was investigated in this paper. The decomposition kinetics parameters were determined via a global optimization of the Kissinger iterative method using the non-isothermal thermogravimetric analysis data. The products and intermediates were synchronously characterized by X-ray diffraction and mass spectrometry. The obtained results indicate that the decomposition process of ammonium sulfate catalyzed by ferric oxide can be divided into four stages of which the activation energies are 123.64, 126.58, 178.77 and 216.99 kJ·mol respectively. The decomposition mechanisms at the first and the fourth stage both belong to Mample power theorem, the second stage belongs to Avrami-Erofeev equation and the third belongs to contracting sphere (volume) equation. The corresponding pre-exponential factors ( ) are calculated simultaneously.

关键词： ammonium sulfate     decomposition kinetics     ferric oxide     thermogravimetric analysis    

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Comparing the adsorption behaviors of Cd, Cu and Pb from water onto Fe-Mn binary oxide, MnO

Wei XU,Huachun LAN,Hongjie WANG,Hongming LIU,Jiuhui QU

《环境科学与工程前沿（英文）》 2015年 第9卷 第3期   页码 385-393 doi: 10.1007/s11783-014-0648-y

摘要： The adsorption potential of FMBO, FeOOH, MnO for the removal of Cd , Cu and Pb in aqueous systems was investigated in this study. Comparing to FMBO and FeOOH, MnO offered a much higher removal capacity towards the three metal ions. The maximal adsorption capacity of MnO for Cd , Cu and Pb were 1.23, 2.25 and 2.60 mmol·g , respectively. And that for FMBO were 0.37, 1.13, and 1.18 mmol·g and for FeOOH were 0.11, 0.86 and 0.48 mmol·g , respectively. The adsorption behaviors of the three metal ions on the three adsorbents were all significantly affected by pH values and heavy metal removal efficiency increased with pH increased. The Langmuir and Freundlich adsorption models were used to describe the adsorption equilibrium of the three metal ions onto the three adsorbents. Results showed that the adsorption equilibrium data fitted well to Langmuir isotherm and this indicated that adsorption of metal ions occurred on the three metal oxides adsorbents limited to the formation of a monolayer. More negative charged of MnO surface than that of FMBO and FeOOH could be ascribed by lower pH of MnO than that of FMBO and FeOOH and this could contribute to more binding sites on MnO surface than that of FMBO and FeOOH. The higher metal ions uptake by MnO than FMBO and FeOOH could be well explained by the surface charge mechanism.

关键词： heavy metals     Fe-Mn binary oxide     manganese dioxide     ferric hydroxide     adsorption    

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Validation of polymer-based nano-iron oxide in further phosphorus removal from bioeffluent: laboratory

Ming HUA, Lili XIAO, Bingcai PAN, Quanxing ZHANG

《环境科学与工程前沿（英文）》 2013年 第7卷 第3期   页码 435-441 doi: 10.1007/s11783-013-0508-1

摘要： The efficient removal of phosphorous from water is an important but challenging task. In this study, we validated the applicability of a new commercially available nanocomposite adsorbent, i.e., a polymer-based hydrated ferric oxide nanocomposite (HFO-201), for the further removal of phosphorous from the bioeffluent discharged from a municipal wastewater treatment plant, and the operating parameters such as the flow rate, temperature and composition of the regenerants were optimized. Laboratory-scale results indicate that phosphorous in real bioeffluent can be effectively removed from 0.92 mg·L to<0.5 mg·L (or even<0.1 mg·L as desired) by the new adsorbent at a flow rate of 50 bed volume (BV) per hour and treatable volume of 3500–4000 BV per run. Phosphorous removal is independent of the ambient temperature in the range of 15°C–40°C. Moreover, the exhausted HFO-201 can be regenerated by a 2% NaOH+ 5% NaCl binary solution for repeated use without significant capacity loss. A scaled-up study further indicated that even though the initial total phosphorus (TP) was as high as 2 mg·L , it could be reduced to<0.5 mg·L , with a working capacity of 4.4–4.8 g·L HFO-201. In general, HFO-201 adsorption is a choice method for the efficient removal of phosphate from biotreated waste effluent.

关键词： bioeffluent     phosphorus removal     nanocomposite adsorbent     hydrated ferric oxide    

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Synthesis of hydroxymethylfurfural and furfural from hardwood and softwood pulp using ferric sulphate

Agneev Mukherjee, Guillermo Portillo-Perez, Marie-Josée Dumont

《化学科学与工程前沿（英文）》 2019年 第13卷 第3期   页码 531-542 doi: 10.1007/s11705-019-1814-3

摘要： Hydroxymethylfurfural (HMF) and furfural are promising chemicals for the creation of a bio-based economy. The development of an inexpensive catalytic system for converting cellulosic biomass into these chemicals is an important step in this regard. Ferric sulphate is a common, cheap and non-toxic Lewis acid that has been used to catalyse reactions such as wood depolymerisation. In this work, ferric sulphate was used to help the production of HMF and furfural from hardwood and softwood pulps. It was found that for hardwood pulp, the use of ferric sulphate alone gave a maximum HMF yield of 31.6 mol-%. The addition of the ionic liquid [BMIM]Cl or HCl as co-catalysts did not lead to an increase in the yields obtained. A prior decationisation step, however, resulted in HMF yields of 50.4 mol-%. Softwood pulp was harder to depolymerise than hardwood, with a yield of 28.7% obtained using ferric sulphate alone. The maximum HMF yield from softwood, 37.9 mol-%, was obtained using a combination of ferric sulphate and dilute HCl. It was thus concluded that ferric sulphate is a promising catalyst for HMF synthesis from cellulosic biomass.

关键词： 5-hydroxymethylfurfural     hardwood     softwood     ferric sulphate     biorefinery    

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Synthesis of p -substituted tetraphenylporphyrins and corresponding ferric complexes with mixed-solvents

Zhicheng SUN, Yuanbin SHE, Rugang ZHONG,

《化学科学与工程前沿（英文）》 2009年 第3卷 第4期   页码 457-461 doi: 10.1007/s11705-009-0169-6

摘要： By using mixed-solvents method, five kinds of -substituted tetraphenylporphyrin compounds [T(-R)PPH, R=NO, Cl, CH, OCH, OH] were synthesized by the condensation of -substituted benzaldehyde with pyrrole in mixed solvents (propionic acid, acetic acid and nitrobenzene), and corresponding ferric complexes [T(-R)PPFeCl] were synthesized in dimethylformamide. The above free base porphyrins were obtained in 30%–50% yields, metalation yields were up to 90% and total yields of ferric complexes were 27%–50%. Effects of reactive conditions, solvents and oxidants on yields of free base porphyrins were investigated and the relevant mechanism was discussed. Structures of the above porphyrin complexes were characterized by ultraviolet-visible (UV-Vis), infrared (IR) and far infrared (FIR) spectroscopy.

关键词： -substituted tetraphenylporphyrin     condensation     -substituted benzaldehyde     dimethylformamide     metalation    

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Enhanced adsorption of phosphate by loading nanosized ferric oxyhydroxide on anion resin

Jing REN,Nan LI,Lin ZHAO,Nanqi REN

《环境科学与工程前沿（英文）》 2014年 第8卷 第4期   页码 531-538 doi: 10.1007/s11783-014-0629-1

摘要： Ferric oxyhydroxide loaded anion exchanger (FOAE) hybrid adsorbent was prepared by loading nanosized ferric oxyhydroxide (FO) on anion exchanger resin for the removal of phosphate from wastewater. TEM and XRD analysis confirmed the existence of FO on FOAE. After FO loading, the adsorption capacity of the hybrid adsorbent increased from 38.70 to 51.52 mg·g . Adsorption processes for both FOAE and anion resin were better fit to the pseudo first order model. Batch adsorption experiments revealed that higher temperature (313K), higher initial phosphate concentration (50 mg·L ) and lower solution pH (pH value of 2) would be more propitious to phosphate adsorption. Competition effect of coexisting anions on phosphate removal can be concluded as sulfate>nitrate>chloride. Freundlich isotherm model can describe the adsorption of phosphate on FOAE more accurately, which indicated the heterogeneous adsorption occurred on the inner-surface of FOAE.

关键词： phosphate removal     adsorption     nanosized ferric oxyhydroxide     anion exchanger    

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Large-scale synthesis of isolated Mn2O3 nanotube/fiber with ferric nitrate as catalyst

ZHANG Aifei, LIU Jiping, L? Guangshu

《化学科学与工程前沿（英文）》 2007年 第1卷 第1期   页码 55-58 doi: 10.1007/s11705-007-0011-y

摘要： Isolated MnO nanotubes and nanofibers were prepared very easily at a large scale with the liquid-phase catalysis method. The MnO nanotubes had dimensions of 30 50 nm (exterior diameter) and 0.2 1.0 ?m (length), approximately. The O nanofibers had dimensions of 10 30 nm (diameter) and 0.4 2.0 ?m (length), approximately. Nano-O with different microstructures including nanotubes, nanofibers and nanoparticles could be selectively synthesized by controlling the contents and proportions of potassium permanganate and ferric nitrate. Ferric nitrate was an ideal catalyst for the preparation of O nanotube/fiber. When cobalt nitrate or nickel nitrate was used as catalyst, only amorphous nano-O was synthesized. X-ray diffraction (XRD) result shows that the O nanotube has a crystalline structure different from o-O, t-O, h-O and ?-O.

关键词： different     nickel     exterior diameter     nanotube     XRD    

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Industrial waste utilization method: producing poly-ferric sulfate (PFS) from sodium-jarosite residue

Zhongguo LI,Wenyi YUAN

《环境科学与工程前沿（英文）》 2015年 第9卷 第4期   页码 731-737 doi: 10.1007/s11783-014-0687-4

摘要： Sodium-jarosite is a type of industrial waste that results from hydrometallurgy and inorganic chemical production. The iron content of jarosite residue may be utilized to produce theoretically the ferrous materials. The difficulty in production of high quality poly-ferric sulfate (PFS) is how to remove impurities contained in jarosite residue. This paper proposes a novel method for disposing sodium-jarosite which can be used to synthesize PFS, a very important reagent for treating waste water. The method consists of a two-step leaching experimental procedures. The first step, pre-leaching process, is to remove impurity metals by strictly controlling the leaching conditions. The acid concentration of acidic water was adjusted according to the content of impurity metals in sodium-jarosite and the leaching temperature was controlled at 25°C. The second step is to decompose sodium-jarosite to provide enough ferric ions for synthesizing PFS, the concentrated sulfuric acid consumption was 0.8 mL·g sodium-jarosite and the leaching temperature was above 60°C. In the experiment, decomposing iron from sulfate sodium-jarosite can take the place of ferric martials for synthesizing PFS. Results show that the PFS synthesized from sodium-jarosite had a high poly-iron complex Fe (SO ) (OH) ·20H O. Further, the PFS product’s specifications satisfied the national standard of China.

关键词： sodium-jarosite residue     utilization     poly-ferric sulfate (PFS)    

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A randomized, controlled, open label non-inferiority trial of intravenous ferric carboxymaltose versus

《医学前沿（英文）》 doi: 10.1007/s11684-023-1001-2

摘要： Iron deficiency (ID) and ID anemia (IDA) pose significant public health concerns in China. Although iron sucrose (IS) treatment is well-established in the country, ferric carboxymaltose (FCM) offers the advantage of higher doses and fewer infusions. This open label, randomized, controlled, non-inferiority trial was conducted at multiple sites in China to compare the outcomes of FCM (maximum of 2 doses, 500 or 1000 mg iron) and IS (up to 11 infusions, 200 mg iron) treatments in subjects with IDA. The primary endpoint was the achievement of hemoglobin (Hb) response (an increase of ≥2 g/dL from baseline) within 8 weeks, whereas secondary endpoints included changes in Hb, transferrin saturation, and serum ferritin levels. Among the 371 randomized subjects, a similar percentage of subjects treated with FCM and IS achieved Hb-response (FCM 99.4%, IS 98.3%), thereby confirming the non-inferiority of FCM compared with IS (difference 1.12 (−2.15, 4.71; 95% confidence interval (CI))). Furthermore, a significantly higher proportion of FCM-treated subjects achieved early Hb-response at Week 2 (FCM 85.2%, IS 73.2%; difference 12.1 (3.31, 20.65; 95% CI)). Additionally, the increase in TSAT and serum ferritin levels from baseline was significantly greater at all time points for FCM-treated subjects. The safety profiles of FCM and IS were comparable, with the exception of transient hypophosphatemia and pyrexia, which are consistent with FCM’s known safety profile. In conclusion, FCM proves to be an efficacious treatment for IDA, providing faster Hb-response and correction of ID with fewer administrations than IS.

关键词： iron deficiency     anemia     intravenous iron     ferric carboxymaltose     iron sucrose     Hb response     early response    

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Cuprous oxide/copper oxide interpenetrated into ordered mesoporous cellulose-based carbon aerogels for

《化学科学与工程前沿（英文）》 2023年 第17卷 第7期   页码 918-929 doi: 10.1007/s11705-023-2305-0

摘要： The casual discharge of dyes from industrial settings has seriously polluted global water systems. Owing to the abundance of biomass resources, preparing photocatalysts for photocatalytic degradation of dyes is significant; however, it still remains challenging. In this work, a cuprous oxide/copper oxide composite was interpenetrated onto carbon nanosheets of cellulose-based flexible carbon aerogels (Cu2O/CuO@CAx) via a simple freeze-drying-calcination method. The introduction of the carbon aerogel effectively prevents the aggregation of the cuprous oxide/copper oxide composite. In addition, Cu2O/CuO@CA0.2 has a larger specific surface area, stronger charge transfer capacity, and lower recombination rate of photogenerated carriers than copper oxide. Moreover, Cu2O/CuO@CA0.2 exhibited high photocatalytic activity in decomposing methylene blue, with a degradation rate reaching up to 99.09% in 60 min. The active oxidation species in the photocatalytic degradation process were systematically investigated by electron spin resonance characterization and poisoning experiments, among which singlet oxygen played a major role. In conclusion, this work provides an effective method for preparing photocatalysts using biomass resources in combination with different metal oxides. It also promotes the development of photocatalytic degradation of dyes.

关键词： carbon aerogel     photocatalysis     dye degradation     biomass     cuprous oxide/copper oxide    

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Mechanical properties and microstructure of multilayer graphene oxide cement mortar

《结构与土木工程前沿（英文）》 2021年 第15卷 第4期   页码 1058-1070 doi: 10.1007/s11709-021-0747-3

摘要： This study reports on the effects of multilayer graphene oxide (MGO) on compressive strength, flexural strength, and microstructure of cement mortar. The cement mortar was prepared with type P. II. 52.5 Portland cement, standard sand, and MGO. Four mixes were prepared with inclusion of MGO (0%, 0.02%, 0.04%, and 0.06% by weight of cement). The testing result shows that the compressive of GO-cement mortar increased by 4.84%–13.42%, and the flexural strength increased by 4.37%–8.28% at 3 d. GO-cement mortar’s compressive strength and flexural strength at 7 d increased by 3.84%–12.08% and 2.54%–13.43%, respectively. MGO made little contribution to the increases of compressive strength and flexural strength of cement mortar at 28 d. The results of X-ray diffraction (XRD), scanning electron microscope (SEM), and nitrogen (N2) adsorption/desorption tests show that the types of hydration products and crystal grain size did not change after adding MGO. Still, it can help to improve the microstructure of the cement mortar via regulating hydration products and can provide more condensed cores to accelerate hydration. Furthermore, the regulating action of MGO for the microstructure of cement mortar at an early age was better than that at 28 d.

关键词： graphene oxide     cement     mortar     mechanical properties     microstructure    

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Plasma spray coating on interconnector toward promoted solid oxide fuel cells and solid oxide electrolysis

《能源前沿（英文）》 doi: 10.1007/s11708-023-0901-9

摘要： Interconnector is a critical component to construct solid oxide cells (SOCs) stack. Oxidation of metallic interconnectors and Cr poisoning caused by oxidation are important factors that lead to long-term performance degradation of SOCs. Coating on the interconnector surface is an important approach to inhibit the oxidation and Cr migration of the interconnector. Herein, (La0.75Sr0.25)0.95MnO3–δ (LSM) and Mn1.5Co1.5O4 (MCO) are used to fabricate the coatings of interconnector. Two advanced thermal spray technology, atmospheric plasma spraying (APS) and low-pressure plasma spray (LPPS), are adopted for the coating preparation. The electrochemical performance, rising and cooling cycle stability, and Cr diffusion inhibition performance of the coatings are tested and evaluated. The result indicates that MCO can generate more uniform and denser coatings than LSM. In addition, MCO coatings prepared by LPPS shows the best electrochemical performance, rising and cooling cycle stability, and Cr diffusion inhibition. The initial area specific resistance (ASR) is 0.0027 Ω·cm2 at 800 °C. After 4 cooling cycle tests, the ASR increases to 0.0032 Ω·cm2 but lower than other samples. Meanwhile, the relative intense of Cr at the interface of SUS430 with MCO coatings fabricated by LPPS is lower than that of MCO fabricated by APS after 4 rising and cooling cycle operations, showing more favorable Cr diffusion inhibition performance.

关键词： interconnector coating     plasma spray     electrochemical performance     Cr diffusion inhibition     solid oxide cells (SOCs)    

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Ammonia adsorption on graphene and graphene oxide: a first-principles study

Yue PENG, Junhua LI

《环境科学与工程前沿（英文）》 2013年 第7卷 第3期   页码 403-411 doi: 10.1007/s11783-013-0491-6

摘要： Motivated by the recent realization of graphene sensor to detect gas molecules that are harmful to the environment, the ammonia adsorption on graphene or graphene oxide (GO) was investigated using first-principles calculation. The optimal adsorption and orientation of the NH molecules on the graphene surfaces were determined, and the adsorption energies ( ) as well as the Mulliken charge transfers of NH were calculated. The for the graphene are small and seem to be independent of the sites and orientations. The surface epoxy or hydroxyl groups can promote the adsorption of NH on the GO; the enhancement of the for the hydroxyl groups is greater than that for the epoxy groups on the surface. The charge transfers from the molecule to the surfaces also exhibit the same trend. The Br?nsted acid sites and Lewis acid sites could stably exist on the GO with surface hydroxyl groups and on the basal, respectively.

关键词： graphene oxide     first-principles calculations     NH3 adsorption    

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Development of oxide dispersion strengthened ferritic steels with and without aluminum

Jae Hoon LEE

《能源前沿（英文）》 2012年 第6卷 第1期   页码 29-34 doi: 10.1007/s11708-012-0178-x

摘要： Pure Fe, Cr, Al, Ti elemental powders and pre-alloyed Y O powder were processed by high energy mechanical milling. The compositions of the mixed powders are designed as Fe-18Cr-0.2Ti-0.35Y O and Fe-18Cr-5Al-0.2Ti-0.35Y O in weight percent. The as-milled powders were consolidated by hot extrusion at 1423 K. The dispersed oxide particles were identified to be titania+ yttria for Al-free oxide dispersion strengthened (ODS) steel and alumina+ yttria for Al-added ODS steel, respectively. The ultimate tensile strength of Al-free ODS steel was higher than that of Al-added ODS steel over the temperature range of 298–973 K, because of the difference in number density and size of thermally stable oxide particles dispersed in both steel matrices. The strength in the longitudinal direction was lower than that in the transverse direction, probably due to anisotropy of the microstructure with elongated grains in the hot-extrusion direction for the 18%Cr-ODS steels with and without 5%Al.

关键词： oxide dispersion strengthened (ODS) steel     milling     extrusion     aluminum     yttria    

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标题 作者 时间 类型 操作

Fabrication and catalytic performance of meso-ZSM-5 zeolite encapsulated ferric oxide nanoparticles for

Zhenheng Diao, Lushi Cheng, Wen Guo, Xu Hou, Pengfei Zheng, Qiuyueming Zhou

期刊论文

Thermal decomposition mechanism of ammonium sulfate catalyzed by ferric oxide

Xingfu SONG, Jingcai ZHAO, Yunzhao LI, Ze SUN, Jianguo YU

期刊论文

Comparing the adsorption behaviors of Cd, Cu and Pb from water onto Fe-Mn binary oxide, MnO

Wei XU,Huachun LAN,Hongjie WANG,Hongming LIU,Jiuhui QU

期刊论文

Validation of polymer-based nano-iron oxide in further phosphorus removal from bioeffluent: laboratory

Ming HUA, Lili XIAO, Bingcai PAN, Quanxing ZHANG

期刊论文

Synthesis of hydroxymethylfurfural and furfural from hardwood and softwood pulp using ferric sulphate

Agneev Mukherjee, Guillermo Portillo-Perez, Marie-Josée Dumont

期刊论文

Synthesis of p -substituted tetraphenylporphyrins and corresponding ferric complexes with mixed-solvents

Zhicheng SUN, Yuanbin SHE, Rugang ZHONG,

期刊论文

Enhanced adsorption of phosphate by loading nanosized ferric oxyhydroxide on anion resin

Jing REN,Nan LI,Lin ZHAO,Nanqi REN

期刊论文

Large-scale synthesis of isolated Mn2O3 nanotube/fiber with ferric nitrate as catalyst

ZHANG Aifei, LIU Jiping, L? Guangshu

期刊论文

Industrial waste utilization method: producing poly-ferric sulfate (PFS) from sodium-jarosite residue

Zhongguo LI,Wenyi YUAN

期刊论文

A randomized, controlled, open label non-inferiority trial of intravenous ferric carboxymaltose versus

期刊论文

Cuprous oxide/copper oxide interpenetrated into ordered mesoporous cellulose-based carbon aerogels for

期刊论文

Mechanical properties and microstructure of multilayer graphene oxide cement mortar

期刊论文

Plasma spray coating on interconnector toward promoted solid oxide fuel cells and solid oxide electrolysis

期刊论文

Ammonia adsorption on graphene and graphene oxide: a first-principles study

Yue PENG, Junhua LI

期刊论文

Development of oxide dispersion strengthened ferritic steels with and without aluminum

Jae Hoon LEE

期刊论文